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The MagLab is funded by the National Science Foundation and the State of Florida.

Biological Solids MAS NMR

Sensitive triple-resonance Low-E 1HXY MAS probes are available to users at 900, 800 and 600 MHz.

The Low-E technology was developed at the MagLab to provide maximum sensitivity of direct detection in CP and double-CP experiments, while protecting biological samples from rf-induced heating. A suite of 2D and 3D MAS experiments (DARR, NCA, NCO, NCOCX, etc.) allows for spectral assignment and structural elucidation of labeled proteins. Several 1HXY detection modes are available.

Details

Available Spectrometers

The following instruments at AMRIS facility are available for this technique:

The following instruments at NMR facility are available for this technique:

The following probes are available for this technique:

  • 1.5 GHz Low-E static 1H–X probe (NHMFL #57) with interchangeable sample coils
  • 900 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #42)
  • 800 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #53)
  • 750 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #50)
  • 750 MHz Low-E 4.0 mm MAS 1H–X probe (NHMFL #29)
  • 600 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #47)
  • 600 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #40)

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Last modified on 06 October 2023

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