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Terahertz EPR Spectroscopy in the High-Homogeneity 36T Series-Connected Hybrid Magnet

New instrumentation allows electron magnetic resonance experiments to be performed in the lab’s flagship 36 T Series-Connected Hybrid magnet, unlocking exceptionally high-resolution EMR spectra at the highest magnetic fields.


Probing Metal Organic Frameworks with 17O NMR at 35.2 T

Metal-organic frameworks (MOFs) are porous materials with high surface areas that can host a variety of different guest molecules, leading to applications in catalysis, drug delivery, chemical separation, fuel cells, and data storage. In order to design better MOFs, knowledge of their molecular-level structures is crucial. At the MagLab, the highest-field NMR spectrometer in the world was used to probe the complex structures of MOFs both "as built" and as they exist when other "guest" molecules are inserted inside the framework.


Structure of Boron-Based Catalysts from 11B Solid-State NMR at 35.2T

Measurements performed at the National High Magnetic Field Laboratory provide unique insight into molecular structure of next-generation catalysts for the production of the widely used industrial chemical, propene.


17O Labeling Reveals Paired Active Sites in Zeolite Catalysts

Zeolite catalysts are critical to generating the molecules that provide the building blocks of society’s energy and materials needs. Discerning a clear atomic-level picture of the active sites remains challenging for most current technologies, but here we show that solid-state nuclear magnetic resonance (ssNMR) methods coupled with ultra-high magnetic field instruments, can and has provided extremely useful information for catalyst development.


Solid-State 17O NMR for Studies of Organic and Biological Molecules

Chemists are rarely able to use oxygen NMR to determine molecular structures, since 17O is an extremely challenging nucleus to observe. This work provides a mechanism for obtaining a complete set of 17O NMR parameters for a glucose molecule, paving the way for researchers to consider 17O NMR as a new spectroscopic tool. 


Unraveling the Mysteries of the Platinum Group Elements with 103Rh Solid-State NMR Spectroscopy

Rhodium (Rh) is one of the most costly and scarce platinum group elements; however, it is of great importance in many technologies including catalytic converters, electronics, and medical devices. Here ultra-high magnetic field instruments and new NMR methodology at the MagLab unlocked access to perform 103Rh solid-state nuclear magnetic resonance, a technique that can study the molecular structures of Rh-containing materials.


National MagLab Racks up New Record with Hybrid Magnet

Combining tremendous strength with a high-quality field, the MagLab’s newest instrument promises big advances in interdisciplinary research.


New NMR Director Takes the Helm

As head of nuclear magnetic resonance at the MagLab's Tallahassee headquarters, Rob Schurko hopes to expand capabilities and build new magnets.


"Water Wires" May Play Bigger Role in Cell Functions

New insights challenge current understanding of how ion transport through some cell membranes works.


NIH Invests in MagLab Biomedical Advances

Improving technology for research of biomolecules and advancing our understanding of health and disease.


MagLab Scientist Honored for Contributions to Nuclear Magnetic Resonance

MagLab NMR Facility Director Rob Schurko was awarded the Vold Prize for his contributions to the field of solid-state NMR over the past 25 years.


Homogeneity: At the MagLab, It’s About More Than Milk

What is homogeneity and why is it so important to scientists? Learn how homogeneous magnets make data clearer by milking the magnetic field strength for all it's worth. 


Crossing a Mack Truck With a Ferrari

Two MagLab teams tried marrying vastly different technologies to build a new type of magnet: the Series Connected Hybrid. Decades later, has the oddball pairing panned out?



Last modified on 10 August 2022