This probe delivers the highest mass sensitivity of any probe at any frequency in the world. For more information about how our liquid-state spectrometers may meet your mini-/micro-sample needs, please contact James Rocca. Generally speaking, our 600-MHz instruments equipped with cryogenically-cooled radio-frequency (RF) probes will provide you with the best sensitivity for proton(1H)-detected spectra. Both spectrometers have commercial 5-mm indirect-detection cryogenic probes. Additionally, there are occasionally available unique, prototype high-temperature-superconducting (HTS) cryogenic "RF micro-probes" that may be more suitable for your sample.
If you are already familiar with Bruker's TopSpin software or Agilent’s VNMR-J software, then Mr. Rocca can provide a check-out for you on either spectrometer. Also contact him if you require training for solution NMR on any of of these systems, or prefer to simply have an operator provided for your sample analysis on one of the spectrometers.
The following spectrometers are available for this technique:
- 800 MHz 63 mm NMR Magnet #3 (Gainesville)
- 800 MHz 54 mm Cryo Bruker Avance III (Gainesville)
- 600 MHz 54 mm NMR System – Cryo Probe (Gainesville)
- 600 MHz 54 mm NMR System - Cold Probe (Gainesville)
The following probes are available for this technique:
- 1.5-mm HTS Probe (see article in Journal of Magnetic Resonance)
Images
Click on an image for more detail.
https://nationalmaglab.org/user-facilities/nmr-mri/nmr-mri-measurement-techniques/hts-probe-for-natural-products#sigProIdb74515e2a5
Staff Contact
- James Rocca (Gainesville)