Biological Solids MAS NMR

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Sensitive triple-resonance Low-E ¹HXY MAS probes are available to users at 900, 800 and 600 MHz. The Low-E technology was developed at the MagLab to provide maximum sensitivity of direct detection in CP and double-CP experiments, while protecting biological samples from rf-induced heating. A suite of 2D and 3D MAS experiments (DARR, NCA, NCO, NCOCX, etc.) allows for spectral assignment and structural elucidation of labeled proteins. Several ¹HXY detection modes are available.

The following instruments are available for this technique:

36 Tesla, 40 mm Bore Series Connected Hybrid Magnet (Cell 14) (Tallahassee)
900 MHz 105 mm NMR Magnet (Tallahassee)
830 MHz 31 mm NMR Magnet (Tallahassee)
800 MHz 63 mm NMR Magnet #1 (Tallahassee)
800 MHz 63 mm NMR Magnet #2 (Tallahassee)
800 MHz 63 mm NMR Magnet #3 (AMRIS) (Gainesville)
750 MHz 89 mm NMR Magnet (Gainesville)
600 MHz 89 mm NMR Magnet #1 (Tallahassee)
600 MHz 89 mm NMR Magnet #2 (Tallahassee)
600 MHz 51 mm NMR Magnet (Gainesville)
500 MHz 54 mm NMR System (Gainesville)
500 MHz 89 mm NMR Magnet for Solid State (Tallahassee)

The following probes are available for this technique:

1.5 GHz Low-E static 1H–X probe (NHMFL #57) with interchangeable sample coils
900 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #42)
800 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #53)
750 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #50)
750 MHz Low-E 4.0 mm MAS 1H–X probe (NHMFL #29)
600 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #47)
600 MHz Low-E 3.2 mm MAS 1H–X–Y probe (NHMFL #40)

Contacts

Last modified on 14 May 2020