600 MHz 54 mm NMR System – Cold Probe

600 MHz 54 mm NMR system – cold probe. 600 MHz 54 mm NMR system – cold probe.

This Agilent VNMRS-600 spectrometer is managed by the University of Florida's AMRIS Facility, but it is located in UF's Chemistry Department.

It can be equipped with a unique 1.5-mm Cold Probe having RF coils made of a High Temperature Superconductor (HTS). That micro-probe has a typical sample volume of about 35 micro-liters, and it has cryogenically-cooled 1H and 13C preamplifiers. It is often used for small samples typical of isolated natural products. The system also has available a commercial 5-mm HCN Cold Probe with cryogenically-cooled 1H and 13C preamplifiers, which therefore has high sensitivity for both 1H and 13C.

Details

  • Specs

  • Techniques & Capabilities

  • Probes

  • MHz: 600
  • Field: 14.1 tesla, actively shielded
  • Bore size: 54 mm
  • Console: Agilent VNMRS (DD1)
  • Homogeneity: 1 ppb
  • VNMR-J 4.0 Software, 7700-CS CryoBay
  • Open for users who would pay for magnet time: Yes

Diffusion

Solution State

  • 1.5 mm HTS Cold Probe; 1H, 13C; Z-Gradient
  • 5 mm Cold Probe; 1H, 13C, 15N; Z-Gradient

Images

View the embedded image gallery online at:
https://nationalmaglab.org/user-facilities/nmr-mri/nmr-instruments/agilent600-coldprobe-amris#sigProIdc6b218b5fa

Staff Contact

For more information please contact James Rocca.

Last modified on 1 July 2021
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