600 MHz 89 mm MAS DNP System

600 MHz 89 mm MAS DNP System 600 MHz 89 mm MAS DNP System

This instrument is located at the MagLab's Tallahassee headquarters.

The increased sensitivity of MAS DNP allows high resolution solid state NMR spectroscopy to be used for many previously inaccessible systems. Our Bruker DNP spectrometer utilizes a 394 GHz gyrotron to produce a strong microwave field to enhance NMR polarization.

Request time for this magnet.

Details

  • Specs

  • Techniques & Capabilities

  • Probes

  • Field: 14.1 tesla
  • Bore diameter: 89 mm
  • ±1% field sweep range (±128 mT)
  • Console: Bruker Avance III running TOPSPIN 3.2
  • 3 rf channels, 1 kW amplifier for 1H/19F, and two 1 kW amplifiers for X and Y-nuclei
  • 3.2 mm magic-angle spinning probe
  • Cooling cabinet with continuous liquid N2 supply
  • Gyrotron microwave source with quasi-optic stable
  • Funded in part by NIH S10 OD018519 (magnet and console), and NSF CHE-1229170 (gyrotron)

  • Bruker 3.2 mm HXY low-temperature (100 K) DNP MAS probe

Image

User Procedures

Contact

For more information please contact Frederic Mentink-Vigier, Thierry Dubroca or Zhehong Gan.

Last modified on 14 January 2021

Magnet Schedule for 600 MHz 89 mm MAS DNP System

* Denotes Offsite Participants

Dates Facility Instruments Experiment
1-25-2021 to 1-29-2021 NMR 600 MHz, 89 mm bore MAS DNP Structural and interaction study of collagen protein in native bone and cartilage through dynamic nuclear polarization Neeraj Sinha (PI) — Centre of Bio-Medical Research (CBMR)
Participants
  • Sungsool Wi — National High Magnetic Field Laboratory
2-1-2021 to 2-5-2021 NMR 600 MHz, 89 mm bore MAS DNP Chlamydomonas reinhardtii cell-wall and whole cell glycan architecture studied by high-field and DNP Solid-State NMR Isabelle Marcotte (PI) — University of Quebec at Montreal
Participants
  • Frederic Mentink — National High Magnetic Field Laboratory
  • Tuo Wang* — Louisiana State University
  • Faith Scott — National High Magnetic Field Laboratory
  • Alex Kirui* — Louisiana State University